Title:
Small-scale synthesis of laboratory reagents with reaction modeling
Author:
Lerner, Leonid.
ISBN:
9781439813133
Publication Information:
Boca Raton : CRC Press, 2011.
Physical Description:
xv, 217 p., [12] p. of col. plates : ill.
Contents:
ch. 1. Safety in the laboratory -- ch. 2. Sodium -- ch. 3. Potassium -- ch. 4. Lithium -- ch. 5. Cesium -- ch. 6. Lithium hydride and sodium hydride -- ch. 7. Bromine -- ch. 8. Aluminum bromide -- ch. 9. Lithium aluminum hydride -- ch. 10. Triethylaluminum and diethylaluminum bromide -- ch. 11. Hydrazine sulfate and alcoholic hydrazine hydrate -- ch. 12. Sodium and potassium azide -- ch. 13. Potassium t-butoxide and potassium hydride -- ch. 14. Carbon disulfide -- ch. 15. Chlorine -- ch. 16. Carbon tetrachloride -- ch. 17. Bis-trichloromethyl carbonate (triphosgene) -- ch. 18. Phosphorus pentachloride -- ch. 19. Phosphorus oxychloride -- ch. 20. Sulfur trioxide and oleum -- ch. 21. Thionyl chloride and chlorosulfonic acid.
Abstract:
"The in-lab preparation of some chemical reagents provides a number of advantages over purchasing commercially-prepared samples. This volume contains a detailed description of methods for the rapid and reliable synthesis of many useful reagants that are otherwise difficult to obtain. It provides spectroscopic analyses of products, presents the thermodynamic/kinetic data of reactions, and offers a thorough analysis of the purity of the final products. Enhanced by useful diagrams and photographs, this text is a valuable reference for researchers in small or remote laboratories"-- Provided by publisher.
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