Part A Introduction -- Molecular Heterogeneity of Polyolefins -- Analytical Methods for Polyolefins -- Part B Crystallization-Based Fractionation Techniques -- Temperature Rising Elution Fractionation -- Crystallization Analysis Fractionation -- Crystallization Elution Fractionation -- Part C Column-Based Chromatographic Techniques -- Multidetector Size Exclusion Chromatography -- Solvent Gradient Interaction Chromatography -- Temperature Gradient Interaction Chromatography -- Two-Dimensional Liquid Chromatography -- Part D Field-Flow Fractionation -- Fundamentals -- Application of Field-Flow Fractionation of Polyolefins -- Analysis of Polyolefins by Asymmetric Flow FFF -- Conclusions and Future Trends.