Part 1 Methodology of power-consuming preparation of nanostructured materials -- Methodology of thermal transformations -- Photo- and radiolytic methods -- Electrochemical methods -- Mechanochemical methods of nanomaterials preparation -- Part 2 The chemical transformations in inorganic matrices -- The peculiarities of structure of inorganic matrices -- Chemical transformations of guest in inorganic matrix -- Systems with crystal matrices -- Reactions in inorganic carrier of high dispersity -- The peculiarities of chemical transformations in sol-gel synthesis.- Part 3 The chemical transformations in organic matrices -- The routes of organometallic compounds decomposition in organic polymer matrices -- Stabilization of polynuclearic metalloclusters and nanoparticles with microencapsulation -- Self-organization of nanoparticles of core-shell structure at the decomposition of metal-containing precursors -- A solid-phase thermolysis of metal-containing monomers and polymers -- The novel approaches to the formation of nanostructured materials -- The preparation of novel layer structures as a route of nanoceramics synthesis -- Thermal transformations of unsaturated metal carboxylates -- Frontal regimes in the preparation of metallopolymer nanocomposites.